STUDY OF GROWTH KINETICS, CHARACTERIZATION AND OPTICAL PROPERTIES OF ELECTRODEPOSITED CUINSE2 THIN FILMS.
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Author(s):
H. R. KULKARNI
Vol - 8, Issue- 2 ,
Page(s) : 61 - 68
(2017 )
DOI : https://doi.org/10.32804/IRJMST
Abstract
CuInSe2 thin films were prepared by using pulsed electrodeposition technique on stainless steel substrates in galvanostatics mode from an aqueous acidic bath containing CuSO4, InCl3 and SeO2. The kinetics of growth of the film was studied. The deposition parameters like concentration of electrolyte, time of deposition, current density and pH of electrolyte bath are optimized. The X-ray Diffraction (XRD) and Electron Dispersive Spectra (EDS) analysis of the deposited film with optimized condition showed presence of polycrystalline nature. The surface morphology was studied with the help of Scanning Electron Microscope (SEM) shows that the deposited films are well adherent and grains are uniformly distributed over the surface of substrate.
- N. G. Patel., Solid State Electrochem. 35:1269 (1992).
- K. Y. Rajpure, C. D. Lokhande and C. H. Bhosale. Mater. Chem. Phy 252:51 (1997)
- V. L. Mathe, K. Y. Rajpure and C. H.Bhosale Bull. Mater.Sci. 22:927 (1999).
- H. J. Goldsmid and J. E. Giutornich, M. M. Kalia., Solar energy 24: 435 (1980).
- R. Janam, N. N. Rao, O. Srivastava, Journal of Physics D: Applied Physics 22 (1989) 1153.
- S. Bereznev, J. Kois, I. Golovtsov, A. Öpik, E. Mellikov, Thin Solid Films 511-512 (2006) 425.
- O. Savadogo, Solar Energy Materials and Solar Cells 52 (1998) 361.
- L. Djellal, S. Omeiri, A. Bouguelia, M. Trari, Journal of Alloys and Compounds 476 (2009) 584
- G. Razzini, L. P. Bicelli, M. Arfelli, B. Scrosati, Journal of Electroanalytical Chemistry and Interfacial Electrochemistry 208 (1986) 85
- T. Edamura, J. Muto, Journal of Materials Science: Materials in Electronics 5 (1994) 275.
- N. Stratieva, E. Tzvetkova, M. Ganchev, K. Kochev, I. Tomov, Solar Energy Materials and Solar Cells 45 (1997) 87.
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